Template-free synthesis of high degree crystallinity zeolite Y with micro–meso–macroporous structure

High temperature synthesis of high silica zeolite Y with good crystallinity in the presence of N-methylpyridinium iodide.

A novel synthetic route is designed, employing both high temperature and a nontoxic organic structure-directing agent (SDA), for the synthesis of high silica zeolite Y. The N-methylpyridinium used as an organic SDA is stable during the synthesis, and the high silica zeolite Y shows high hydrothermal stability and good catalytic performance, as well as excellent adsorptive properties.

Hydrothermal Synthesis of Aligned Hydroxyapatite Nanorods with Ultra-High Crystallinity

Hydroxyapatite nanorods aligned with ultrahigh crystallinity and high-yield were successfully synthesized through a hydrothermal approach. In this experiment, a new composition of cetyltrimethylammonium bromide ((CH3(CH2)15N+(CH3)3Br-) was designated as CTAP)/Ca(NO3)2/(NH4)2HPO4/NaOH and distilled water under hydrothermal condition, to synthesize single crystalHAp nanorods with diameter of 20 ±...

Synthesis of zeolite NaA nano-crystalls; effect of synthesis parameters on crystallinity and crystal size

Abstract In this work hydrothermal synthesis of zeolite NaA crystals with a composition of Al2O3:aSiO2:bNa2O:cH2O was investigated. Effects of SiO2/Al2O3, Na2O/Al2O3 and H2O/Al2O3 ratios and crystallization temperature and time were studied on crystallinity and crystal size of zeolite NaA crystals. It was tried to understand the interactions between these parameters. The crystal species o...

Template-Free Synthesis of Monoclinic BiVO4 with Porous Structure and Its High Photocatalytic Activity

Monoclinic BiVO₄ photocatalysts with porous structures were synthesized by a two-step approach without assistance of any templates. The as-prepared samples were characterized by X-ray diffraction pattern (XRD), scanning electron microscopy (SEM), Brunauer-Emmett-Teller (BET), ultraviolet-visible (UV-vis) diffuse reflectance spectroscopy (DRS), photocurrent responses, and electrochemical impedan...

Synthesis of a Zeolite Column with a Monolithic Microhoneycomb Structure Using the Ice Template Method